An optimized LBF enables solubilization of the entire therapeutic dose and maintains the drug in solubilized state throughout the digestion process.
\nTo speed up LBF development, we have produced tools to guide you at each stage of development:
\n1 – methods for saturation solubility screening
\n2 – database of solubility of drugs in common pharmaceutical excipients
\n3 – methods for miscibility and dispersability testing
\n4 – miscibility table
\n5 – in vitro lipolysis procedure
\n6 – guideline for preclinical studies
\nExposed to environmental stress, the skin’s barrier function is altered, facilitating the penetration of irritants, and increasing Trans Epidermal Water Loss (TEWL). As a result, the skin becomes dry and presents sensitivity, associated with redness and a stinging sensation. There is a growing need for mild, soothing texture ingredients that reduce skin sensitivity to aggression and enable the use of skincare and make-up products without reaction and discomfort.
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publications"},"content":{"rendered":"","protected":false},"excerpt":{"rendered":"","protected":false},"author":9,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"_yoast_wpseo_title":"An exhaustive list of all the scientific publications from Gattefossé experts","_yoast_wpseo_metadesc":"Find out the scientific articles and posters written by our pharmaceutical scientists about lipid-based excipients and formulation technologies."},"categories":[63],"tags":[],"acf":{"component":"Brochures","title":"Gattefossé publications","introduction":"Find below the list of all publications (articles and posters) of Gattefossé scientists.Posters are available to download after log-in.","":false,"content":[{"wysiwyg":"Lipids and polymers in pharmaceutical technology: Lifelong companions
\nSolubilisation behaviour of poorly water-soluble drugs during digestion of solid SMEDDS
\nLipid-based nanosuspensions for oral delivery of peptides, a critical review
\nSelf-emulsifying peptide drug delivery systems: How to make them highly mucus permeating
\nCompritol® 888 ATO: a sustained release lipid matrix for once a day aceclofenac tablets
\n\n"},{"wysiwyg":"
Interest of carriers for the development of solid self-emulsifying drug delivery systems
\nBibliography on Gattefossé’s products. 2004-2005 review.
\nSolubilisation behaviour of poorly water-soluble drugs during digestion of solid SMEDDS
\nLipid-based nanosuspensions for oral delivery of peptides, a critical review
\nSelf-emulsifying peptide drug delivery systems: How to make them highly mucus permeating
\nCompritol® 888 ATO: a sustained release lipid matrix for once a day aceclofenac tablets
\nInterest of carriers for the development of solid self-emulsifying drug delivery systems
\nBibliography on Gattefossé’s products. 2004-2005 review.
\nDevelopment of immediate release pellets of poorly soluble compounds using Gelucire® 44/14
\nCamille Dumont
\nCamille Dumont, Vincent Jannin, Sandrine Bourgeois, Ana Beloqui, Véronique Préat, Hatem Fessi
\nPoster PBP 2021
\n\n"},{"wysiwyg":"Camille Dumont, Ana Beloqui, Cédric Miolane, Sandrine Bourgeois, Véronique Préat, Hatem Fessi, Vincent Jannin
\nInternational Journal of Pharmaceutics, Volume 586, 30 August 2020
\nThis study aimed to evaluate the potential of Hydrophobic Ion Pairing combined with Solid Lipid Nanoparticles (SLN) and Nanostructured Lipid Carriers (NLC) to improve peptide transport across the intestinal border using Caco-2 cell monolayers (enterocyte-like model) and Caco-2/HT29-MTX co-cultured monolayers (mucin-secreting model).
\nThis study showed that hydrophobic ion pairing enabled high encapsulation efficiency of peptide in SLN and NLC. The lipid-based nanocarriers were highly internalized by Caco-2 cell monolayers and were able to cross the mucus barrier (Caco-2/HT29-MTX cell model). However, the peptide intestinal transport was limited by an extensive release from the carriers.
\n\n\n
\n"},{"wysiwyg":"
Dr Camille Dumont
\nAmerican Pharma Review, May-June 2020 issue, pp 69-75
\nIn this comprehensive article, the author describes the latest tools available to develop solid lipid nanoparticles: how to prepare and characterize solid lipid nanoparticles, how to evaluate encapsulation efficiency and intestinal permebility.
\n\n"},{"wysiwyg":"Camille Dumont, Vincent Jannin, Cédric Miolane, Quentin Lelong, Jean-Pierre Valour, Sebastien Urbaniak, Hatem Fessib, Sandrine Bourgeois
\nJournal of Drug Delivery Science and Technology (article in press)
\nIn this study, the authors developed a protocol to produce reproducible solid lipid nanoparticles by high pressure homogeneization. The possibility to encapsulate peptides was also investigated.
\n\n"},{"wysiwyg":"Camille Dumont, Ana Beloqui, Sandrine Bourgeois, Véronique Préat, Hatem Fessi, Vincent Jannin
\nPoster CRS 2019
\n\n"},{"wysiwyg":"Camille Dumont, Sandrine Bourgeois, Hatem Fessib, Pierre-Yves Dugas, Vincent Jannin
\nInternational Journal of Pharmaceutics, Volume 565, 30 June 2019, Pages 409-418
\n\n"},{"wysiwyg":"Camille Dumont, Sandrine Bourgeois, Hatem Fessi, Vincent Jannin
\nDumont C., Jannin V., Beloqui A., Préat V., Fessi H.c, Bourgeois S.
\nIn this study the authors obtained solid lipid nanoparticles using high pressure homogeneization, in which leuprolide was included as an ion pair. The nanoparticles were shown to be internalized by Caco-2 and Caco-2/HT29-MTX cell monolayers.
\n\n"},{"wysiwyg":"Published online October 2017
\nEuropean Journal of Pharmaceutical Sciences , Volume 111, 1 January 2018, Pages 91-95
\nIn this study, solid lipid nanoparticles (SLN) of glyceryl dibehenate are produced by two methods and evaluated for digestion using the in vitro lipolysis test.
\nDuring tablet and capsule production, lubricants are necessary to improve powder flow and reduce friction and adherence. Lubrication is a critical step since over- or underlubrication is responsible for many production and quality issues. Therefore, lubricant type, quantity, and conditions of use are critical parameters to take into account when developing a formulation.
\n\nGattefossé lubricants are recommended for challenging formulations. They are also able to resolve production and quality issues due to these qualities:
\n\n
W/O (water-in-oil) emulsions are becoming more and more preferred in the personal care space, particularly regarding color cosmetics and sun care. In color cosmetics, W/O foundations offer better water resistance, long-wear, and high coverage – all the performance qualities a consumer desires – compared to O/W (oil-in-water) formulations. And though W/Si (water-in-silicone) formulations may offer great performance and texture, they do not qualify as natural makeup, making them a less desirable option among younger shoppers. When it comes to sun care, consumers are moving towards mineral options. Sunscreen launches containing zinc oxide increased by 45% from 2014-15 to 2018-19 in North America(1). Zinc oxide is easier to formulate in a W/O than an O/W system. In fact, most inorganic sunscreens are either anhydrous or W/O formulations.
\nHowever, formulating can be easier said than done, as there are many challenges that come with making a stable W/O product. W/O systems are more sensitive to other ingredients and require more energy in their processing to ensure stability. There are two key factors to consider when it comes to W/O formulation: oil polarity and electrolyte addition, which may not have any influence or not even be necessary for O/W formulations.
\n\n
\n The emulsifier you choose has distinctive characteristics that will help you determine the profile of your other ingredients. One trait to consider, that is often overlooked, is polarity. If you are using a more polar emulsifying agent, then your oil phase should consist of more polar oils. Some medium to high polarity oils include C12-15 alkyl benzoate, caprylic/capric triglycerides, octyldodecyl myristate, castor oil, and coco-glycerides, among countless others. On the other hand, if the emulsifier is not very polar, then your oil phase should be more comprised of apolar oils, such as alkanes like squalane, or undecane, tridecane, or silicones if preferred.
\n\n
\n
\n The stability of W/O emulsions can be improved by adding a proper concentration of inorganic salts, such as CaCl2, NaCl, MgCl2, and MgSO4, in the aqueous phase(2). Adding salts to a W/O emulsion inhibits Ostwald ripening, which is where smaller droplets diffuse and deposit themselves onto larger droplets.
\n\n Inorganic salts can also lower the interfacial tension at an oil-water interface, thereby improving stability against coalescence and sedimentation(2).
\n
\n Attractive forces exist within the dispersed phase and can increase their collision frequency(2). This can lead to either coalescence or sedimentation. However, by adding electrolytes to the system, you can lower the attractive forces between water droplets to ensure stability.
\nNeedless to say, electrolytes are absolutely necessary to ensure a stable formula, maintaining the smaller droplet sizes in a consistent, even dispersion.
\n\n
\n
Emulium® Illustro is Gattefossé’s gold-winning, naturally derived, high performing, W/O emulsifier that can help you create a natural, stable, and sensorial make-up, sun care, or skincare product! You will notice that this ingredient has a very large, polar head group and long lipophilic chains that also have polar bonds, as seen by the hydroxide and ester groups:
\n
Because of these polar properties, Emulium® Illustro is more compatible with medium to high polarity oils. But since we’ve engineered this ingredient to be highly compatible and flexible, you may still incorporate apolar oils at certain percentage levels. And as for electrolytes, our R&D team found this ingredient to work very well with 2% MgSO4 or 1% of MgSO4 and NaCl. Check out this video to see how you can make a 2-min emulsion using Emulium® Illustro!
\n\n
\n
\n
\n
(1) Mintel GNPD
\n(2) Qiaomei Zhu, Yijun Pan, Xin Jia, Jinlong Li, Min Zhang, Lijun Yin. Review on the Stability Mechanism and Application of Water‐in‐Oil Emulsions Encapsulating Various Additives. (2019)
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\nSpecial attention is given to a selective harvest of the flowers (upper buds only), so that the plant can be used by local population for other applications, especially for cooking.
\nEfficacy validated through complete substantiation studies:
\nTargeted solution for firming body and facial care
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Formulations must be robust to ensure drug release over time and avoid dose-dumping. Lipid-based matrices are water-insoluble and do not swell or erode when in contact with aqueous media. When used as sustained-release agents, they form an inert matrix from which the drug diffuses slowly.
• Drug release is a function of diffusion, which enables simple product design and offers both straightforward modulation of drug release and high reproducibility. • Tablets are biopharmaceutically robust as the lipid matrix is not sensitive to physiological variations (e.g., pH, digestive processes, alcohol level). • Agents are suitable for a wide range of processing techniques, including direct compression, granulation, melt coating, hot melt extrusion, and capsule molding.
\nSome APIs present poor organoleptic properties; therefore, taste or odor need to be masked. Others are sensitive to water, oxidation, or temperature and need to be protected to maintain stability. Certain lipid excipients are used in melt processes to effectively protect the API from degradation or mask taste and odor.
\n\n
• thermoplastic behavior conducive to processes used (high shear coating, hot melt coating, granulation, extrusion, and capsule molding) • solvent-free process • chemically inert—highly compatible with other excipients in the formulation • plastic deformation for high resistance to compaction • lipid coating that does not impact bioavailability
Suppocire® bases comprise chemically stable fatty acid esters with a narrow melting range. Their physicochemical properties provide numerous formulation and manufacturing advantages, including optimized solidification properties and straightforward scale-up with low, medium, and high throughput manufacturing equipment. Careful selection of the right Suppocire® base ensures optimal physicochemical stability and drug delivery properties, as defined by European Pharmacopeia requirements. In addition, Suppocire® formulations are usually simple binary mixtures of the API dissolved or dispersed in the suppository base. They do not require additional excipients to enhance performance, quality, or stability. Step 1: Suppocire® melting Suppocire® pellets are heated at 20 °C above the melting point—indicated in the product technical data sheet—while stirring to ensure the base is thoroughly melted and perfectly homogenized. Step 2: API addition The API is added at a temperature above the recrystallization temperature of the base, generally 30–45 °C. Stirring continues during addition of the API to ensure homogeneity.
Step 3: Blister filling The melted, homogenized mixture is poured into the mold at a specific temperature, as determined by a thermorheogram.
A thermorheogram plots viscosity versus temperature and allows you to find the optimal mold or blister filling temperature during production. Since viscosity is a function of the specific formulation ingredients, a thermorheogram is necessary for each formulation. Gattefossé has a thermorheogram for each grade of product in the product page section.
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This is the simplest process for the production of tablets. It consists of three main steps: powder blending, lubrication, and compression. Atomized lipid excipients are used as lubricants or modified-release agents in direct compression.
\n\nAdvantages of lipid excipients in direct compression:
\nRange of functional excipients for direct compression:
\n\n
Sticking issue
\nSticking during tableting is a relatively common problem. It is often attributable to tooling and machine setup. However, the formulation, active ingredient, and excipients can play an important role. We conducted an in-house study to evaluate the cause of punch adhesion or “sticking,” which occasionally occurs during the compression of powder formulations containing Compritol® 888 ATO. Our study concludes that sticking is primarily due to a combination of factors, including formulation with a “sticky” API and use of ingredients with reduced interparticle bonding capacity.
\nContact Gattefossé for the full study report.
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Find out quickly the excipient you are looking for! This updated version has been enriched with the precedence of use of our excipients.
\n"},{"wysiwyg":"\nInterested in solubility and bioavailability enhancement? Sustained-release? Taste-masking? Lubricant?This brochure will help you choose the appropriate excipient!
\n"},{"wysiwyg":"\nEmulsifiers, thickeners, solubilizers and penetration enhancers will have no secret for you after reading this brochure!
\n"},{"wysiwyg":"\nDiscover our wide range of suppository bases and how Gattefossé expertise can speed up your development!
\nFind out about our solutions for cannabinoid drug products.
\n"},{"wysiwyg":"\nFind out our solutions for oral, topical and rectal dosage forms suitable for pediatric patients.
\nFind out our solutions for domestic and farm animals!
\n"},{"wysiwyg":"Compritol® 888 ATO many advantages in sustained release are highlighted and its use in single or dual SR matrix is explained.
\n"},{"wysiwyg":"Inert, robust and efficient: 3 words that summarize the outstanding benefits of Compritol® 888 ATO
\n"},{"wysiwyg":"All you should know about this water soluble surfactant for successful lipid-based formulations
\n"},{"wysiwyg":"All you should know about this functional oil for successful lipid-based formulations
\n"}],"box_links":[{"link":"https://www.gattefosse.com/pharmaceuticals-product-finder/product-finder-pharmaceutical/","title":"Access our product finder","external_link":false,"image":"https://www.gattefosse.com/wordpress/wp-content/uploads/2016/11/tableau_noir_624x221px.jpg"},{"link":"https://www.gattefosse.com/pharmaceuticals-formulation-technologies/formulation-technologies/","title":"Understand how to use our excipients","external_link":false,"image":"https://www.gattefosse.com/wordpress/wp-content/uploads/2016/11/technologies_196x143px.jpg"}],"useful_links":[],"":false,"introduction":"Click on the descriptions to open brochures.","vignets_articles":[{"image":{"id":26682,"alt":"","title":"product catalogue technical spotlight 2","caption":"","description":"","mime_type":"image/jpeg","url":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2.jpg","width":106,"height":150,"sizes":{"thumbnail":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2-106x150.jpg","thumbnail-width":106,"thumbnail-height":150,"medium":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2.jpg","medium-width":106,"medium-height":150,"medium_large":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2.jpg","medium_large-width":106,"medium_large-height":150,"large":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2.jpg","large-width":106,"large-height":150,"post-thumbnail":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2.jpg","post-thumbnail-width":106,"post-thumbnail-height":150,"twentyfourteen-full-width":"https://www.gattefosse.com/wordpress/wp-content/uploads/2019/05/product-catalogue-technical-spotlight-2.jpg","twentyfourteen-full-width-width":106,"twentyfourteen-full-width-height":150}},"title":"Product catalogue","text":"Find out quickly the excipient you are looking for! This updated version has been enriched with the precedence of use of our excipients.
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René-Maurice Gattefossé, Henri-Marcel Gattefossé, and Emile Mahler all strongly believed in the power of collaborative work and nurtured strong relationships with professional partners, academicians, and collaborators. Today, the company works at perpetuating this legacy and is proud of its rich corporate culture, influenced by the characters of its founders.
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\n\n
Gattefossé invests in its employees to keep them at the forefront of their fields.
\n
In accordance with French legislation, Gattefossé has calculated its Professional Equality Index for its major entity in France, Gattefossé SAS: at the end of 2020, the result is 89/100 :
\n\n
\n
\n
\n
“My priorities are clearly linked to further securing the future of Gattefossé by expanding to new locations, pursuing R&D efforts, and forging additional strategic alliances.
These goals are closely connected to my vision, summarized by the following tenets of our company’s family culture:
\n\n
Jacques Moyrand and his wife, Sophie Gattefossé-Moyrand, also created the Gattefossé Foundation in 2008, with the desire to perpetuate Gattefossé’s founders’ vision and values by serving a long-term general interest.
The Foundation’s purpose is to promote the scientific and clinical use of essential oils as a complementary therapeutic approach to health, primarily within hospital settings.
\n\n\n
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Thus, 3DP was implemented to explore the feasibility of 3DP technology for the development of solid lipid-based formulations. 3DP was applied for the development of solid self-micro-emulsifying drug delivery systems (S-SMEDDS) with defined surface area to volume (SA/V) ratios to control the formulation dispersion kinetics.","link":"https://attendee.gotowebinar.com/recording/6494783709893239308","category":[{"term_id":73,"name":"Oral delivery","slug":"oral-delivery","term_group":0,"term_taxonomy_id":73,"taxonomy":"category","description":"","parent":72,"count":0,"filter":"raw"}]},{"id":"","image":{"id":20407,"alt":"","title":"agenda-canabis","caption":"","description":"","mime_type":"image/jpeg","url":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis.jpg","width":739,"height":644,"sizes":{"thumbnail":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis-150x150.jpg","thumbnail-width":150,"thumbnail-height":150,"medium":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis-300x261.jpg","medium-width":300,"medium-height":261,"medium_large":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis.jpg","medium_large-width":474,"medium_large-height":413,"large":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis.jpg","large-width":474,"large-height":413,"post-thumbnail":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis-672x372.jpg","post-thumbnail-width":672,"post-thumbnail-height":372,"twentyfourteen-full-width":"https://www.gattefosse.com/wordpress/wp-content/uploads/2017/02/agenda-canabis-739x576.jpg","twentyfourteen-full-width-width":739,"twentyfourteen-full-width-height":576}},"title":"Strategies for cannabinoids for topical formulations","description":"This webinar will focus on topical dosage forms containing cannabinoids. 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Palm oil dominates the worldwide oil market. It is used in food, energy, industrial uses, and of course, personal care. Yet its impact on deforestation and biodiversity have rightfully raised concerns – primary forest in Indonesia, the main producer of palm oil, is rapidly being eroded.
The rapid and unplanned culture of oil palm has deeply affected the biodiversity of Southeast Asia. As demand for palm oil has grown, deforestation and endangerment of local animal species has become a growing problem.
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To combat these environmental concerns, the Roundtable for Sustainable Palm Oil (RSPO) was created in 2004 with a goal of making sustainable cultivation of palm oil, respectful of people and the environment, the norm instead of the exception. RSPO certified sustainable palm oil has been produced to stringent environmental and social criteria.
\n\n\n
1 – Book & Claim – Certified palm producers register output with GreenPalm and are granted certificates for each ton of sustainable palm oil produced. Manufacturers bid for those certificates, thereby supporting the production of sustainable palm oil.
\n2 – Mass Balance (MB) – Allows for a mixture of sustainable and conventional palm oil. Overall volumes of each are carefully monitored
\n3 – Segregated SG – Allows for certified palm oil to come from a number of producers, but guarantees that the entire quantity of palm oil is sustainably produced.
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